二溴化二丁锡(996-08-7)核磁图(¹³CNMR)

Mass

MS-NW-9896          
dibutyltin dibromide
C8H18Br2Sn          (Mass of molecular ion:    392)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       2.4
      29.0      14.6
      39.0       2.1
      41.0      18.4
      55.0       1.7
      56.0       2.4
      57.0     100.0
      58.0       4.8
     119.0       1.3
     120.0       1.2
     121.0       1.5
     153.0       1.1
     155.0       1.6
     195.0       2.0
     196.0       1.0
     197.0       5.0
     198.0       2.1
     199.0       7.4
     200.0       1.1
     201.0       4.8
     203.0       1.4
     252.0       1.0
     254.0       2.4
     255.0       1.7
     256.0       3.5
     257.0       1.2
     258.0       2.2
     289.0       1.7
     291.0       2.7
     293.0       2.1
     311.0       1.0
     312.0       1.0
     313.0       1.2
     331.0       1.7
     333.0       5.4
     334.0       2.7
     335.0       9.6
     336.0       2.9
     337.0       9.3
     338.0       1.3
     339.0       4.7
     341.0       1.6

Assign. Shift(ppm) A 1.907 B 1.777 C 1.432 D 0.959

     Hz     ppm     Int.

    771.24   1.930    119
    764.04   1.912    229
    755.86   1.892    220
    744.63   1.864     39
    724.24   1.813     91
    716.92   1.794    143
    715.21   1.790    129
    709.23   1.775    179
    708.37   1.773    169
    701.29   1.755    140
    693.85   1.737     57
    590.70   1.479     59
    583.25   1.460    186
    575.68   1.441    289
    568.36   1.423    301
    561.16   1.405    192
    553.96   1.387     60
    390.38   0.977    589
    383.06   0.959   1000
    375.61   0.940    531