CAS:

分子式:C13H18O

分子量: 190.28142

Mass

MS-NW-7719          
1-methyl-2-phenylcyclohexanol
C13H18O             (Mass of molecular ion:    190)

   Source Temperature: 270 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       1.5
      18.0       1.2
      27.0       5.9
      28.0       1.8
      29.0       3.2
      31.0       1.1
      39.0       8.0
      40.0       1.0
      41.0       8.8
      43.0      58.3
      44.0       1.7
      45.0       2.7
      50.0       1.7
      51.0       6.2
      52.0       1.9
      53.0       3.0
      54.0       1.0
      55.0       3.6
      57.0       2.0
      58.0      22.7
      59.0       4.9
      63.0       3.3
      64.0       1.3
      65.0       6.6
      67.0       1.7
      68.0       1.2
      69.0       1.5
      71.0      75.1
      72.0       5.2
      75.0       1.0
      76.0       1.3
      77.0      10.5
      78.0       9.1
      79.0       6.0
      80.0       2.1
      81.0       8.6
      85.0       3.3
      89.0       2.6
      90.0       1.2
      91.0     100.0
      92.0      17.4
      93.0       1.6
      94.0       2.3
      97.0       1.2
      99.0       6.0
     102.0       1.9
     103.0       8.1
     104.0      32.7
     105.0      13.2
     106.0       1.3
     107.0       1.8
     115.0      11.9
     116.0       3.7
     117.0      21.2
     118.0       4.2
     119.0       2.6
     120.0       1.0
     127.0       1.4
     128.0       4.8
     129.0      19.1
     130.0      79.7
     131.0      12.3
     132.0      25.4
     133.0       3.6
     134.0       1.1
     143.0       8.9
     144.0       4.4
     145.0       1.1
     147.0       6.4
     148.0       1.1
     157.0       7.9
     158.0       1.2
     172.0      68.3
     173.0      10.5
     174.0       4.7
     175.0       3.5
     190.0      10.5
     191.0       1.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₁₈ O	0.05 ml : 0.5 ml CDCl₃
1-methyl-2-phenylcyclohexanol

    Assign.     Shift(ppm)

      A             7.29
      B             7.28
      C             7.26
      D             2.471
      E             2.038
      F             1.81
      G             1.71
      J             1.59
      K             1.46
      L             1.33
      M             0.959

     Hz     ppm     Int.

   2926.15   7.322     61
   2924.93   7.319     49
   2924.07   7.317     50
   2922.36   7.313     36
   2920.17   7.307    108
   2918.95   7.304    173
   2917.60   7.301    101
   2916.50   7.298     85
   2915.41   7.295     73
   2912.84   7.289    234
   2911.74   7.286    359
   2910.64   7.283    275
   2906.98   7.274    134
   2904.79   7.269    467
   2904.05   7.267    363
   2901.73   7.261     93
   2900.02   7.257    337
   2898.07   7.252    500
   2895.39   7.245    107
   2892.94   7.239    148
   2891.60   7.236    230
   2889.65   7.231    300
   2888.31   7.228    187
   2887.57   7.226    147
   2886.47   7.223    378
   2884.89   7.219     69
   2883.67   7.216    116
   2882.32   7.213    115
   2881.23   7.210    263
   2878.30   7.203     66
   2876.22   7.197     59
   2874.39   7.193     88
   2872.68   7.188     43
    996.34   2.494     58
    992.92   2.485     60
    983.40   2.461     68
    979.98   2.453     67
    823.85   2.062     47
    820.19   2.053     50
    810.67   2.029     55
    807.01   2.020     55
    738.65   1.849     36
    736.82   1.844     42
    735.96   1.842     37
    734.99   1.840     34
    733.76   1.837     32
    733.28   1.835     31
    730.10   1.827     31
    727.54   1.821     55
    723.88   1.812     88
    721.31   1.805     67
    716.80   1.794     38
    714.84   1.789     35
    712.89   1.784     61
    711.06   1.780     57
    710.57   1.778     57
    709.35   1.775     64
    707.03   1.770     33
    702.03   1.757     40
    698.36   1.748     43
    688.96   1.724     36
    685.30   1.715     55
    671.75   1.681     30
    645.63   1.616     65
    642.94   1.609     72
    640.38   1.603     47
    638.92   1.599     47
    637.45   1.596     41
    636.60   1.593     37
    636.35   1.593     37
    633.54   1.586     45
    632.32   1.583     53
    630.74   1.579     44
    629.27   1.575     51
    627.32   1.570     31
    625.73   1.566     30
    599.85   1.501     50
    586.55   1.468     81
    582.40   1.458     62
    573.24   1.435     42
    542.60   1.358     40
    538.94   1.349     53
    529.66   1.326     36
    526.00   1.317     48
    383.42   0.960   1000

in CDCl3

liquid film

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