L-Histidine hydrochloride
L-Histidine hydrochloride атрибут
Температура плавления: |
240-245 °C (dec.) |
альфа: |
[α]D20 +7.0~+10.0°(c=2,HCl) |
температура хранения: |
Inert atmosphere,Room Temperature |
Справочник по базе данных CAS: |
1007-42-7(CAS DataBase Reference) |
Заявления о рисках и безопасности
Заявления о безопасности |
22-24/25 |
РИДАДР |
UN 1789 8/PG 3 |
WGK Германия |
3 |
F |
3-10 |
L-Histidine hydrochloride химические свойства, назначение, производство
Методы очистки
The dihydrochloride crystallises from water or aqueous EtOH and is washed with acetone, then diethyl ether. Alternatively convert it to the histidine di-(3,4-dichlorobenzenesulfonate) salt by dissolving 3,4-dichlorobenzenesulfonic acid (1.5g/10mL) in the aqueous histidine solution with warming, and then the solution is cooled in ice. The resulting crystals (m 280o dec) can be recrystallised from 5% aqueous 3,4-dichlorobenzenesulfonic acid, then dried over CaCl2 under vacuum, and washed with diethyl ether to remove Purification of Biochemicals — Amino Acids and Peptides excess reagent. The dihydrochloride can be regenerated by passing the solution through a Dowex-1 (Cl-form) ion-exchange column. The solid is obtained by evaporation of the solution on a steam bath or better in a vacuum. [Greenstein & Winitz, The Amino Acids Vol 3 p 1976 1961, Beilstein 25/16 V 366.]
L-Histidine hydrochloride препаратная продукция и сырье
сырьё
препарат
L-Histidine hydrochloride поставщик
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