1,1,1-TRIFLUORO-6-METHYLHEPTANE-2,4-DIONE synthesis
- Product Name:1,1,1-TRIFLUORO-6-METHYLHEPTANE-2,4-DIONE
- CAS Number:461-92-7
- Molecular formula:C8H11F3O2
- Molecular Weight:196.17
Yield:461-92-7 19.5%
Reaction Conditions:
Stage #1: trifluoroacetic acid-methyl esterwith sodium hydride in tetrahydrofuran;Inert atmosphere;
Stage #2: 4-methyl-2-pentanone in tetrahydrofuran;Inert atmosphere;
References:
Simunek, Petr;Svobodova, Marketa;Machacek, Vladimir [Journal of Heterocyclic Chemistry,2009,vol. 46,# 4,p. 650 - 655] Location in patent:experimental part
383-63-1
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$10.00/25g
108-10-1
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$12.00/25ml
461-92-7
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$55.00/1g