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1,1-dimethylindan-5,6-diol synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 88 percent / polyphosphoric acid / 15 h / 60 °C
2: 69 percent / Zn; aq. HCl / toluene / 72 h / Heating
3: 9 percent / Me3SiI / acetonitrile / 60 h / 20 °C

References:

Kraft, Philip;Eichenberger, Walter [European Journal of Organic Chemistry,2003,# 19,p. 3735 - 3743]

51458-29-8 Synthesis
5,6-Dimethoxy-1,1-dimethyl-2,3-dihydro-1H-indene

51458-29-8
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1,1-dimethylindan-5,6-diol

97337-98-9
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