Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

1-[2-(1-Piperidyl)phenyl]ethanol synthesis

3synthesis methods
39911-06-3 Synthesis
2'-(1-Piperidinyl)acetophenone

39911-06-3
16 suppliers
$175.00/500mg

-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: pyridine; hydroxyamino hydrochloride / ethanol / 1 h / Inert atmosphere; Reflux
2: pyridine; potassium hexafluoridophosphate; 4-methylbenzenesulfonyl chloride / dichloromethane / 1 h / 0 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C

References:

Ning, Yingtang;Kawahata, Masatoshi;Yamaguchi, Kentaro;Otani, Yuko;Ohwada, Tomohiko [Chemical Communications,2018,vol. 54,# 15,p. 1881 - 1884]