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ChemicalBook CAS DataBase List 1-(2-PYRIDYL)-2-(2-NITROBENZYL)ALKYNE

1-(2-PYRIDYL)-2-(2-NITROBENZYL)ALKYNE synthesis

5synthesis methods
1945-84-2 Synthesis
2-ETHYNYLPYRIDINE

1945-84-2
225 suppliers
$12.00/1g

609-73-4 Synthesis
1-Iodo-2-nitrobenzene

609-73-4
9 suppliers
$10.00/5g

1-(2-PYRIDYL)-2-(2-NITROBENZYL)ALKYNE

155372-21-7
12 suppliers
inquiry

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Yield:155372-21-7 55%

Reaction Conditions:

with bis-triphenylphosphine-palladium(II) chloride;copper(l) iodide;triethylamine;triphenylphosphine in N,N-dimethyl-formamide at 20; for 6 h;Inert atmosphere;Sonogashira coupling;

References:

Ramana, Chepuri V.;Patel, Pitambar;Vanka, Kumar;Miao, Benchun;Degterev, Alexei [European Journal of Organic Chemistry,2010,# 31,p. 5955 - 5966] Location in patent:experimental part