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33539-20-7

1-(3,6-dihydroxy-2-methoxyphenyl)ethanone synthesis

6synthesis methods
Preparation from 2-hydroxy-6-methoxyacetophenone by persulfate oxidation (Elbs reaction) (26–33%).
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Yield:33539-20-7 85%

Reaction Conditions:

with calcium sulfate;copper(l) chloride in ethyl acetate;acetonitrile at 20; for 3 h;Product distribution;Further Variations:;Reaction partners;

References:

Capdevielle, Patrice;Maumy, Michel [Tetrahedron,2001,vol. 57,# 2,p. 379 - 384]

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