1-(3-METHOXY-4-METHYLPHENYL)ETHAN-1-ONE synthesis
- Product Name:1-(3-METHOXY-4-METHYLPHENYL)ETHAN-1-ONE
- CAS Number:3556-81-8
- Molecular formula:C10H12O2
- Molecular Weight:164.2
3556-60-3
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$17.00/1g
3556-81-8
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$45.00/50mg
Yield:3556-81-8 99%
Reaction Conditions:
with hydrogenchloride in CH3 MgI;diethyl ether;
Steps:
P.13 Preparation of Benzylamine Derivative
This 3-methoxy-4-methylcyanobenzene in the amount of 35 grams (238 millimoles) was mixed with 43.5 grams (262 millimoles) of CH3 MgI and then heated under reflux for 4.5 hours in 200 milliliters of diethyl ether. Then, to the reaction product thus obtained, 300 milliliters of 6 Normal hydrochloric acid was added, and the resulting mixture was heated under reflux for 1 hour. A diethyl ether layer was separated, washed with water and then dried over anhydrous sodium sulfate. Subsequently the diethyl ether was distilled away under reduced pressure. Thus, as a product, 39.0 grams (238 millimoles) of 3-methoxy-4-methylacetophenone was obtained (yield, 99%).
References:
US4680054,1987,A
75-16-1
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135754-83-5
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3556-81-8
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3556-60-3
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676-58-4
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$15.00/25ml
3556-81-8
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33414-49-2
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74-88-4
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3556-81-8
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7151-68-0
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3556-81-8
29 suppliers
$45.00/50mg