1,4-di(propynyl)benzene synthesis
- Product Name:1,4-di(propynyl)benzene
- CAS Number:105058-42-2
- Molecular formula:C12H10
- Molecular Weight:154.21
935-14-8
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Yield:105058-42-2 95%
Reaction Conditions:
Stage #1: 1,4-diethynylbenzenewith n-butyllithium in tetrahydrofuran at -78; for 1 h;
Stage #2: methyl iodide at 0 - 20; for 12 h;
References:
Sokolov, Jan;Lizal, Tomas;Sindelar, Vladimir [New Journal of Chemistry,2017,vol. 41,# 14,p. 6105 - 6111]
