1-(4-Pyridyl)heptan-1-one synthesis
- Product Name:1-(4-Pyridyl)heptan-1-one
- CAS Number:32941-30-3
- Molecular formula:C12H17NO
- Molecular Weight:191.27
872-85-5
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 50 percent / conc. aq. H2SO4 / methanol / 19 h / Heating
2: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) THF, hexane, a) from -78 deg C to 0 deg C, 2.5 h, b) RT, 0.5 h
3: 87 percent / formic acid / 1.5 h / 80 °C
References:
Sheldrake [Synthetic Communications,1993,vol. 23,# 14,p. 1967 - 1971]
55-22-1
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32941-30-3
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82736-91-2
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32941-30-3
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