1,5-BIS(4-METHOXYPHENYL)-3-PHENYLFORMAZAN synthesis
2synthesis methods
- Product Name:1,5-BIS(4-METHOXYPHENYL)-3-PHENYLFORMAZAN
- CAS Number:14936-32-4
- Molecular formula:C21H20N4O2
- Molecular Weight:360.41
Yield:14936-32-4 82%
Reaction Conditions:
Stage #1: 2-oxo-3-(phenyl)propionic acidwith sodium hydroxide in water at 0; for 0.5 h;
Stage #2: 4-methoxy-anilinewith hydrogenchloride in water at 0; for 0.166667 h;
Stage #3: with sodium nitrite in water at 0;
References:
Maar, Ryan R.;Barbon, Stephanie M.;Sharma, Neha;Groom, Hilary;Luyt, Leonard G.;Gilroy, Joe B. [Chemistry - A European Journal,2015,vol. 21,# 44,p. 15589 - 15599]
