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1-BroMo-2-(2-propen-1-yloxy)-benzene synthesis

4synthesis methods
-

Yield:60333-75-7 100%

Reaction Conditions:

with potassium carbonate in propan-2-one; for 6 h;Heating / reflux;

Steps:

11.J

Construction of Boc-T105 was accomplished in 10% overall yield starting from 2-bromophenol (105-1, 45 g, 260 mmol).

References:

US2008/194672,2008,A1 Location in patent:Page/Page column 42-43