1-BROMO-3-ETHOXYPROPANE synthesis
- Product Name:1-BROMO-3-ETHOXYPROPANE
- CAS Number:36865-40-4
- Molecular formula:C5H11BrO
- Molecular Weight:167.04
337913-25-4
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Yield:36865-40-4 100%
Reaction Conditions:
with triphenylphosphine in tetrachloromethane;
Steps:
3.A Step A
Step A 3-Bromopropyl Ethyl Ether To a solution of 3-ethoxypropanol (5.0 g, 48 mmol) in carbon tetrachloride (19.1 g, 57.6 mmol) cooled to 0° C. was added triphenylphosphine (15.1 g, 57.6 mmol); this mixture was stirred for 3 hr, filtered through silica gel and evaporated to a residue which was distilled to give and oil (10.98 g). Redistillation of the oil from phosphorous pentoxide gave 3-bromopropyl ethyl ether (8.0 g, 100%): bp 142°-144° C.
References:
US5538966,1996,A
111-35-3
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