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1-broMo-3-(prop-1-ynyl)benzene synthesis

3synthesis methods
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Yield:66952-36-1 98%

Reaction Conditions:

with copper(l) iodide;tetrakis(triphenylphosphine) palladium(0);tetrabutyl ammonium fluoride;triethylamine in tetrahydrofuran;toluene at 20; for 17 h;Schlenk technique;Inert atmosphere;

References:

Pfeifer, Lukas;Gouverneur, Véronique [Organic Letters,2018,vol. 20,# 6,p. 1576 - 1579] Location in patent:supporting information