ChemicalBook CAS DataBase List 1-CHLORO-7-PHENYLHEPTANE

1-CHLORO-7-PHENYLHEPTANE synthesis

6synthesis methods

Product Name:1-CHLORO-7-PHENYLHEPTANE
CAS Number:54636-29-2
Molecular formula:C13H19Cl
Molecular Weight:210.74

108-88-3
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2163-00-0 Synthesis

2163-00-0
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54636-29-2
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Yield:54636-29-2 87%

Reaction Conditions:

Stage #1: toluenewith 3-(chloromethyl)heptane;N,N,N,N,-tetramethylethylenediamine;natrium in hexane;isopropanol at 25; for 0.5 h;Flow reactor;
Stage #2: 1,6-dichlorohexane in tetrahydrofuran;hexane;isopropanol at -20 - 25; for 0.7 h;Flow reactor;

References:

Harenberg, Johannes H.;Reddy Annapureddy, Rajasekar;Karaghiosoff, Konstantin;Knochel, Paul [Angewandte Chemie - International Edition,2022,vol. 61,# 30,art. no. E202203807][Angew. Chem.,2022,vol. 134,# 30] Location in patent:supporting information

98-59-9 Synthesis