1-Fluoro-4-(3-nitrophenyl)benzene synthesis

11synthesis methods

Product Name:1-Fluoro-4-(3-nitrophenyl)benzene
CAS Number:10540-32-6
Molecular formula:C12H8FNO2
Molecular Weight:217.2

645-00-1
9 suppliers
$50.00/1g

1765-93-1 Synthesis

1765-93-1
550 suppliers
$9.00/1g

10540-32-6
11 suppliers
$60.00/100mg

Yield:10540-32-6 99%

Reaction Conditions:

with potassium phosphate tribasic trihydrate in toluene at 100; for 8 h;Inert atmosphere;Suzuki Coupling;

Steps:

8 Example 5: Ni(II)-α-diimine-POP catalyst catalyzes the reaction between iodobenzene and phenylboronic acid

General procedure: Iodobenzene (1.0 mmol, 116 μL), phenylboronic acid (1.1 mmol, 0.134 g), K3PO4·3H2O (2 mmol, 0.533 g), and Ni(II)-α-diimine-POP (52 mg), 2 ml of toluene was added at 100 °C. Stir for 8h under N2. The yield was determined by gas chromatography. Yield: 99%.

References:

CN110229080,2019,A Location in patent:Paragraph 0092-0093; 0106-0111

585-79-5 Synthesis