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TRIS(4-FLUOROPHENYL)BISMUTHINE synthesis

6synthesis methods
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Yield:437-29-6 95 %

Reaction Conditions:

Stage #1: 1-Bromo-4-fluorobenzenewith iodine;magnesium in tetrahydrofuran at 20;Schlenk technique;Inert atmosphere;
Stage #2: bismuth(III) bromide at 20;

References:

Calcatelli, Alessio;Denton, Ross M.;Ball, Liam T. [Organic Letters,2022,vol. 24,# 43,p. 8002 - 8007] Location in patent:supporting information