1-METHYL-3-(METHYLTHIO)-1H-INDOLE synthesis
- Product Name:1-METHYL-3-(METHYLTHIO)-1H-INDOLE
- CAS Number:116442-14-9
- Molecular formula:C10H11NS
- Molecular Weight:177.27
120-72-9
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 2 h / 20 °C / Inert atmosphere
1.2: 2 h / 20 °C / Inert atmosphere
2.1: magnesium bromide / N,N-dimethyl acetamide / 90 °C / Inert atmosphere
References:
Kona, Chandrababu Naidu;Nishii, Yuji;Miura, Masahiro [Organic Letters,2018,vol. 20,# 16,p. 4898 - 4901]
603-76-9
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67-68-5
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$18.00/5g
20277-69-4
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