![](/CAS/GIF/116442-14-9.gif)
1-METHYL-3-(METHYLTHIO)-1H-INDOLE synthesis
- Product Name:1-METHYL-3-(METHYLTHIO)-1H-INDOLE
- CAS Number:116442-14-9
- Molecular formula:C10H11NS
- Molecular Weight:177.27
![Indole](/CAS/20200515/GIF/120-72-9.gif)
120-72-9
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$6.00/25g
![1-METHYL-3-(METHYLTHIO)-1H-INDOLE](/CAS/GIF/116442-14-9.gif)
116442-14-9
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 2 h / 20 °C / Inert atmosphere
1.2: 2 h / 20 °C / Inert atmosphere
2.1: magnesium bromide / N,N-dimethyl acetamide / 90 °C / Inert atmosphere
References:
Kona, Chandrababu Naidu;Nishii, Yuji;Miura, Masahiro [Organic Letters,2018,vol. 20,# 16,p. 4898 - 4901]
![1-Methylindole](/CAS/GIF/603-76-9.gif)
603-76-9
413 suppliers
$18.00/5g
![Dimethyl sulfoxide](/CAS/GIF/67-68-5.gif)
67-68-5
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$15.00/100g
![1-METHYL-3-(METHYLTHIO)-1H-INDOLE](/CAS/GIF/116442-14-9.gif)
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![1-Methylindole](/CAS/GIF/603-76-9.gif)
603-76-9
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$18.00/5g
![Sodium methanesulfinate](/CAS/GIF/20277-69-4.gif)
20277-69-4
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$10.00/1g
![1-METHYL-3-(METHYLTHIO)-1H-INDOLE](/CAS/GIF/116442-14-9.gif)
116442-14-9
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