1-phenyl-1-aminomethylethene synthesis
- Product Name:1-phenyl-1-aminomethylethene
- CAS Number:28144-67-4
- Molecular formula:C9H11N
- Molecular Weight:133.19
3360-54-1
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Yield:28144-67-4 94%
Reaction Conditions:
Stage #1: 3-bromo-2-phenylprop-1-enewith sodium azide in tetrahydrofuran;water at 50; for 2 h;
Stage #2: with triphenylphosphine in tetrahydrofuran;water; for 20 h;
References:
Scheidt, Felix;Neufeld, Jessica;Sch?fer, Michael;Thiehoff, Christian;Gilmour, Ryan [Organic Letters,2018,vol. 20,# 24,p. 8073 - 8076] Location in patent:supporting information
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6006-81-1
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98-83-9
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