1-Propanol, 3-(octadecyloxy)-2-(phenylmethoxy)- synthesis
- Product Name:1-Propanol, 3-(octadecyloxy)-2-(phenylmethoxy)-
- CAS Number:86008-21-1
- Molecular formula:C28H50O3
- Molecular Weight:434.69
112-89-0
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Yield:-
Steps:
Multi-step reaction with 5 steps
1.1: sodium hydride / toluene / Inert atmosphere; Schlenk technique; Reflux
2.1: hydrogenchloride / water; methanol / 2 h / Inert atmosphere; Schlenk technique; Reflux
3.1: pyridine / 16 h / 50 °C / Inert atmosphere; Schlenk technique
4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique
4.2: 20 °C / Inert atmosphere; Schlenk technique
5.1: toluene-4-sulfonic acid / methanol; dichloromethane / 4 h / 20 °C / Inert atmosphere; Schlenk technique
References:
Alam, Md. Maqusood;Hassan, Ahmed H.E.;Lee, Kun Won;Cho, Min Chang;Yang, Ji Seul;Song, Jiho;Min, Kyung Hoon;Hong, Jongki;Kim, Dong-Hyun;Lee, Yong Sup [Bioorganic Chemistry,2019,vol. 84,p. 51 - 62]
1000210-73-0
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629-93-6
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14690-00-7
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544-62-7
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86334-56-7
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