ChemicalBook CAS DataBase List Batyl alcohol

Batyl alcohol synthesis

11synthesis methods

Product Name:Batyl alcohol
CAS Number:544-62-7
Molecular formula:C21H44O3
Molecular Weight:344.57

16725-43-2
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Yield:544-62-7 96%

Reaction Conditions:

with hydrogenchloride in water for 4 h;Reflux;

Steps:

3.4.3. Preparation of the Ether-Glycerol 4a-i by Hydrolysis of Acetal 3a-i
General procedure: To a solution of 4-alkoxymethyl-2,2-dimethyl-1, 3-dioxolane (1.0 eq.) in methanol (approx. 5 mL), HCl (2 M, 2.0 eq.) was added and the solution was heated to reflux for 4 h. After cooling to room temperature, the mixture was poured into water, the organic layers were extracted with ether, dried over Na2SO4 and the solvents were removed under vacuum. The residue was purified by flash chromatography with hexane/ethyl acetate 3/1 v/v.

References:

Pinault, Michelle;Guimaraes, Cyrille;Couthon, Hélène;Thibonnet, Jérôme;Fontaine, Delphine;Chantôme, Aurélie;Chevalier, Stephan;Besson, Pierre;Jaffrès, Paul-Alain;Vandier, Christophe [Marine Drugs,2018,vol. 16,# 4,art. no. 101]

FullText

57-11-4 Synthesis