1-PYRENESULFONYL CHLORIDE synthesis
- Product Name:1-PYRENESULFONYL CHLORIDE
- CAS Number:61494-52-8
- Molecular formula:C16H9ClO2S
- Molecular Weight:300.76
59323-54-5
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$91.00/500mg
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Yield:61494-52-8 80%
Reaction Conditions:
Stage #1: sodium pyrene-1-sulfonatewith hydrogenchloride;thionyl chloride in N,N-dimethyl-formamide at 5; for 3 h;Inert atmosphere;
Stage #2: with hydrogenchloride in diethyl ether at 0;Inert atmosphere;
References:
Yan, Ni;Xu, Zhiyan;Diehn, Kevin K.;Raghavan, Srinivasa R.;Fang, Yu;Weiss, Richard G. [Journal of the American Chemical Society,2013,vol. 135,# 24,p. 8989 - 8999] Location in patent:supporting information
26651-23-0
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129-00-0
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$9.00/1g
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1714-29-0
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$6.00/1g
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