Naphthalene synthesis
- Product Name:Naphthalene
- CAS Number:91-20-3
- Molecular formula:C10H8
- Molecular Weight:128.17
17135-74-9
272 suppliers
$8.00/250mg
91-20-3
509 suppliers
$14.00/25g
Yield:91-20-3 100%
Reaction Conditions:
with sodium tetrahydridoborate;[1,2-bis(diphenylphosphino)ethane]dichloronickel(II) in N,N-dimethyl-formamide at 20; for 18 h;Solvent;
Steps:
Catalytic hydrodehalogenation experiments
General procedure: All reactions were carriedout in air at room temperature. A 50 mL round-bottom flask equippedwith a magnetic stir bar was charged with 280.8 mg (0.90 mmol) of 4,4′ -dibromobiphenyl (or 0.90 mmol of another aryl halide), 0.09 mmol ofcatalyst (10 mole%), 68.1 mg (0.18 mmol, 2.0 eq) of NaBH4 and 6 mL ofDMF (or other solvents) in room temperature. The reaction mixture wasleft to stir overnight for 18 h. Thereafter, 6 mL of deionised water wasadded to stop the reaction by deactivating the excess NaBH4 in themixture.
References:
Fan, Wai Yip;Guek, Sebastian Jun Kai;Ji, Li;Koh, Hwee Ling;Loke, James Wen Liang [Molecular catalysis,2022,vol. 524,art. no. 112310]
7433-79-6
49 suppliers
$103.73/1g
91-20-3
509 suppliers
$14.00/25g
201230-82-2
1 suppliers
inquiry
90-14-2
287 suppliers
$19.00/5g
91-20-3
509 suppliers
$14.00/25g
66-77-3
381 suppliers
$7.00/10g
86-55-5
370 suppliers
$5.00/5g
91-20-3
509 suppliers
$14.00/25g
66-77-3
381 suppliers
$7.00/10g
91-20-3
509 suppliers
$14.00/25g