Naphthalene synthesis
- Product Name:Naphthalene
- CAS Number:91-20-3
- Molecular formula:C10H8
- Molecular Weight:128.17
17135-74-9
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91-20-3
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$14.00/25g
Yield:91-20-3 100%
Reaction Conditions:
with sodium tetrahydridoborate;[1,2-bis(diphenylphosphino)ethane]dichloronickel(II) in N,N-dimethyl-formamide at 20; for 18 h;Solvent;
Steps:
Catalytic hydrodehalogenation experiments
General procedure: All reactions were carriedout in air at room temperature. A 50 mL round-bottom flask equippedwith a magnetic stir bar was charged with 280.8 mg (0.90 mmol) of 4,4′ -dibromobiphenyl (or 0.90 mmol of another aryl halide), 0.09 mmol ofcatalyst (10 mole%), 68.1 mg (0.18 mmol, 2.0 eq) of NaBH4 and 6 mL ofDMF (or other solvents) in room temperature. The reaction mixture wasleft to stir overnight for 18 h. Thereafter, 6 mL of deionised water wasadded to stop the reaction by deactivating the excess NaBH4 in themixture.
References:
Fan, Wai Yip;Guek, Sebastian Jun Kai;Ji, Li;Koh, Hwee Ling;Loke, James Wen Liang [Molecular catalysis,2022,vol. 524,art. no. 112310]
7433-79-6
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91-20-3
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201230-82-2
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90-14-2
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91-20-3
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66-77-3
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86-55-5
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91-20-3
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$14.00/25g
66-77-3
383 suppliers
$7.00/10g
91-20-3
510 suppliers
$14.00/25g