ChemicalBook CAS DataBase List (S)-3-(3-broMophenyl)-4-(4-chlorophenyl)butan-2-one

(S)-3-(3-broMophenyl)-4-(4-chlorophenyl)butan-2-one synthesis

4synthesis methods

Product Name:(S)-3-(3-broMophenyl)-4-(4-chlorophenyl)butan-2-one
CAS Number:1002752-54-6
Molecular formula:C16H14BrClO
Molecular Weight:337.64

Benzenepropanoyl chloride, α-(3-bromophenyl)-4-chloro-

1204241-05-3
0 suppliers
inquiry

676-58-4 Synthesis

676-58-4
276 suppliers
$15.00/25ml

(S)-3-(3-broMophenyl)-4-(4-chlorophenyl)butan-2-one

1002752-54-6
8 suppliers
inquiry

Yield:1002752-54-6 11.5 kg

Reaction Conditions:

Stage #1: C₁₅H₁₁BrCl₂Owith N,O-dimethylhydroxylamine*hydrochloride;potassium carbonate in water at 30; for 1.25 h;Inert atmosphere;Large scale;
Stage #2: methylmagnesium chloride in water;toluene; for 1.5 h;Inert atmosphere;Large scale;

References:

Chen, G-Yi;Frey, Lisa F.;Shultz, Scott;Wallace, Debra J.;Marcantonio, Karen;Payack, Joeseph F.;Vazquez, Enrique;Springfield, Shawn A.;Zhou, George;Liu, Ping;Kieczykowski, Gerard R.;Chen, Alex M.;Phenix, Brian D.;Singh, Utpal;Strine, Jeff;Izzo, Brianne;Krska, Shane W. [Organic Process Research and Development,2007,vol. 11,# 3,p. 616 - 623]

1878-67-7 Synthesis

1878-67-7
326 suppliers
$5.00/5g

1002752-54-6
8 suppliers
inquiry

References

2-(3-bromophenyl)-3-(4-chlorophenyl)propanoic acid

941280-51-9
6 suppliers
inquiry

1002752-54-6
8 suppliers
inquiry

References

104-83-6 Synthesis

104-83-6
372 suppliers
$15.00/50g

1002752-54-6
8 suppliers
inquiry

References