8-Nonenoic acid, 2-aMino-, ethyl ester, hydrochloride, (2S)- synthesis

1synthesis methods

Product Name:8-Nonenoic acid, 2-aMino-, ethyl ester, hydrochloride, (2S)-
CAS Number:1025368-60-8
Molecular formula:C11H22ClNO2
Molecular Weight:235.75

64-17-5 Synthesis

64-17-5
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300831-21-4 Synthesis

8-Nonenoic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, (2S)-

300831-21-4
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$88.00/1g

8-Nonenoic acid, 2-aMino-, ethyl ester, hydrochloride, (2S)-

1025368-60-8
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Yield:-

Reaction Conditions:

with hydrogenchloride at 20; for 2 h;

Steps:

B.B1.1

A stirred solution of (25)-2-[(t-butoxycarbonyl)amino]non-8-enoic acid (ACME Bioscience Inc) (1.00 g, 3.69 mmol) in EtOH (10 ml) was saturated with HCl gas. The mixture was stirred at RT for 2 hours, then concentrated to give the title product (0.85 g). LRMS (ESI) m/z 200.4 [(M+H)⁺; calcd for C₁₁H₂₂NO₂: 200.2].

References:

WO2008/57208,2008,A2 Location in patent:Page/Page column 32