Carbamic acid, N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methylethyl]-, 1,1-dimethylethyl ester synthesis

2synthesis methods

Product Name:Carbamic acid, N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methylethyl]-, 1,1-dimethylethyl ester
CAS Number:1034153-26-8
Molecular formula:C15H23NO4
Molecular Weight:281.35

1034153-28-0 Synthesis

Carbamic acid, N-[(1S)-2-(3-methoxyphenyl)-1-methyl-2-oxoethyl]-, 1,1-dimethylethyl ester

1034153-28-0
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Carbamic acid, N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methylethyl]-, 1,1-dimethylethyl ester

1034153-26-8
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Yield:1034153-26-8 92%

Reaction Conditions:

with aluminum isopropoxide;isopropyl alcohol in toluene at 50; for 16 h;Inert atmosphere;stereoselective reaction;Meerwein-Ponndorf-Verley Reduction;

References:

Hemmerling, Martin;Nilsson, Stinabritt;Edman, Karl;Eirefelt, Stefan;Russell, Wayne;Hendrickx, Ramon;Johnsson, Eskil;K?rrman M?rdh, Carina;Berger, Markus;Rehwinkel, Hartmut;Abrahamsson, Anna;Dahmén, Jan;Eriksson, Anders R.;Gabos, Balint;Henriksson, Krister;Hossain, Nafizal;Ivanova, Svetlana;Jansson, Anne-Helene;Jensen, Tina J.;Jerre, Anders;Johansson, Henrik;Klingstedt, Tomas;Lepist?, Matti;Lindsj?, Martin;Mile, Irene;Nikitidis, Grigorios;Steele, John;Tehler, Ulrika;Wissler, Lisa;Hansson, Thomas [Journal of Medicinal Chemistry,2017,vol. 60,# 20,p. 8591 - 8605]

15761-38-3 Synthesis

15761-38-3
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1034153-26-8
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References