ChemicalBook CAS DataBase List Methyl 3-bromo-2-(bromomethyl)-4,5-dimethoxybenzoate

Methyl 3-bromo-2-(bromomethyl)-4,5-dimethoxybenzoate synthesis

1synthesis methods

Product Name:Methyl 3-bromo-2-(bromomethyl)-4,5-dimethoxybenzoate
CAS Number:1042722-41-7
Molecular formula:C11H12Br2O4
Molecular Weight:368.02

1042722-40-6 Synthesis

Benzoic acid, 3-bromo-4,5-dimethoxy-2-methyl-, methyl ester

1042722-40-6
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Methyl 3-bromo-2-(bromomethyl)-4,5-dimethoxybenzoate

1042722-41-7
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Yield:1042722-41-7 96%

Reaction Conditions:

with N-Bromosuccinimide;2,2'-azobis(isobutyronitrile) in benzene at 80; for 1 h;

References:

Kim, Joa Kyum;Kim, Young Ha;Nam, Ho Tae;Kim, Bum Tae;Heo, Jung-Nyoung [Organic Letters,2008,vol. 10,# 16,p. 3543 - 3546] Location in patent:supporting information; experimental part