Benzoic acid, 4-[4-[(5,5-dimethyl-2-oxocyclohexyl)methyl]-1-piperazinyl]-, 1,1-dimethylethyl ester synthesis

1synthesis methods

Product Name:Benzoic acid, 4-[4-[(5,5-dimethyl-2-oxocyclohexyl)methyl]-1-piperazinyl]-, 1,1-dimethylethyl ester
CAS Number:1044598-92-6
Molecular formula:C24H36N2O3
Molecular Weight:400.55

50-00-0 Synthesis

50-00-0
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$10.00/25g

187669-28-9 Synthesis

4-Piperazin-1-yl-benzoic acid tert-butyl ester

187669-28-9
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$34.00/250mg

4255-62-3 Synthesis

4255-62-3
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$10.00/1g

Benzoic acid, 4-[4-[(5,5-dimethyl-2-oxocyclohexyl)methyl]-1-piperazinyl]-, 1,1-dimethylethyl ester

1044598-92-6
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Yield:1044598-92-6 53%

Reaction Conditions:

with hydrogenchloride in tert-butyl alcohol; for 3 h;Reflux;Mannich reaction;

References:

Wang, Guangjun;Zhang, Hushan;Zhou, Jing;Ha, Chengyong;Pei, Duanqing;Ding, Ke [Synthesis,2008,# 15,art. no. F04408SS,p. 2398 - 2404] Location in patent:experimental part