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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 3,3-DiMethyl-1-[difluoro(phenylsulfonyl)Methyl]-1,2-benziodoxole
1052174-67-0

3,3-DiMethyl-1-[difluoro(phenylsulfonyl)Methyl]-1,2-benziodoxole synthesis

1synthesis methods
175786-58-0 Synthesis
1,2-Benziodoxole, 1-(acetyloxy)-1,3-dihydro-3,3-dimethyl

175786-58-0
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[difluoro(phenylsulfonyl)Methyl]triMethyl-Silane

536975-50-5
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3,3-DiMethyl-1-[difluoro(phenylsulfonyl)Methyl]-1,2-benziodoxole

1052174-67-0
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Yield:1052174-67-0 71%

Reaction Conditions:

tetrabutylammonium triphenyldifluorosilicate in N,N-dimethyl-formamide at -16; for 18 h;

References:

Zhang, Wei;Zhu, Jieming;Hu, Jinbo [Tetrahedron Letters,2008,vol. 49,# 34,p. 5006 - 5008]