BETA-OXO-4-CHLORO-BENZENEPROPANOIC ACID 1,1-DIMETHYLETHYL ESTER synthesis
- Product Name:BETA-OXO-4-CHLORO-BENZENEPROPANOIC ACID 1,1-DIMETHYLETHYL ESTER
- CAS Number:106970-98-3
- Molecular formula:C13H15ClO3
- Molecular Weight:254.712
540-88-5
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122334-37-6
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106970-98-3
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Yield:106970-98-3 421 mg
Reaction Conditions:
Stage #1: acetic acid tert-butyl esterwith n-butyllithium;N-ethyl-N,N-diisopropylamine in tetrahydrofuran;hexane at -78; for 0.5 h;
Stage #2: 4-chloro-N-methoxy-N-methylbenzamide in tetrahydrofuran;hexane at -78; for 1 h;
References:
Yin, Qi;Wen, Xiaolu;Chen, Yiwei;Gong, Xiangnan;Hu, Lin [Organic Letters,2021,vol. 23,# 19,p. 7529 - 7534] Location in patent:supporting information
2033-24-1
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75-65-0
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74-11-3
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$5.00/1g
106970-98-3
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122-01-0
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$13.00/25g
106970-98-3
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