ChemicalBook CAS DataBase List Carbonothioic acid, S-ethyl O-((5-methyl-2-oxo-1,3-dioxol-4-yl)methyl) ester

Carbonothioic acid, S-ethyl O-((5-methyl-2-oxo-1,3-dioxol-4-yl)methyl) ester synthesis

1synthesis methods

Product Name:Carbonothioic acid, S-ethyl O-((5-methyl-2-oxo-1,3-dioxol-4-yl)methyl) ester
CAS Number:1121795-67-2
Molecular formula:C8H10O5S
Molecular Weight:218.23

91526-18-0 Synthesis

4-(Hydroxymethyl)-5-methyl-1,3-dioxol-2-one

91526-18-0
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2941-64-2 Synthesis

2941-64-2
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Carbonothioic acid, S-ethyl O-((5-methyl-2-oxo-1,3-dioxol-4-yl)methyl) ester

1121795-67-2
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Yield:1121795-67-2 77%

Reaction Conditions:

with pyridine in diethyl ether at 0 - 20; for 19 h;

References:

Rais, Rana;Jan?a?ík, Andrej;Tenora, Luká?;Nedelcovych, Michael;Alt, Jesse;Englert, Judson;Rojas, Camilo;Le, Anne;Elgogary, Amira;Tan, Jessica;Monincová, Lenka;Pate, Kelly;Adams, Robert;Ferraris, Dana;Powell, Jonathan;Majer, Pavel;Slusher, Barbara S. [Journal of Medicinal Chemistry,2016,vol. 59,# 18,p. 8621 - 8633]