ChemicalBook CAS DataBase List (2-TRIMETHYLSTANNANYL-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER

(2-TRIMETHYLSTANNANYL-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER synthesis

5synthesis methods

Product Name:(2-TRIMETHYLSTANNANYL-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER
CAS Number:114552-32-8
Molecular formula:C14H23NO2Sn
Molecular Weight:356.05

3422-01-3 Synthesis

3422-01-3
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7646-78-8 Synthesis

7646-78-8
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(2-TRIMETHYLSTANNANYL-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER

114552-32-8
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Yield:114552-32-8 51%

Reaction Conditions:

Stage #1: tert-butyl phenylcarbamatewith tert.-butyl lithium in diethyl ether;pentane at -40 - 0; for 3.5 h;Inert atmosphere;
Stage #2: tin(IV) chloride in diethyl ether;pentane at -78 - 0; for 6 h;Inert atmosphere;

References:

Maslah, Hichem;Skarbek, Charles;Gourson, Catherine;Plamont, Marie-Aude;Pethe, Stéphanie;Jullien, Ludovic;Le Saux, Thomas;Labruère, Rapha?l [Angewandte Chemie - International Edition,2021,vol. 60,# 45,p. 24043 - 24047][Angew. Chem.,2021,vol. 133,# 45,p. 24245 - 24249] Location in patent:supporting information

3422-01-3 Synthesis

3422-01-3
93 suppliers
$10.00/1g