2-(4-Methyoxyphenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine synthesis

7synthesis methods

Product Name:2-(4-Methyoxyphenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine
CAS Number:1159803-53-8
Molecular formula:C17H15BN2O
Molecular Weight:274.12

5720-07-0 Synthesis

5720-07-0
454 suppliers
$6.00/5g

479-27-6 Synthesis

479-27-6
361 suppliers
$6.00/10g

2-(4-Methyoxyphenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

1159803-53-8
16 suppliers
$45.00/50mg

Yield:1159803-53-8 95%

Reaction Conditions:

at 150; for 0.25 h;Microwave irradiation;Sealed tube;

Steps:

4.2 General procedures for the synthesis of compounds 5a-f

General procedure: The1,8-diaminonaphthalene (0.4 mmol) and boronic acid (0.4 mmol) were added to a microwave tube and sealed with a microwave septum. The tube was shaken to mix and subjected to microwave irradiation at 150 °C for 15 min (150 W) under a closed system. ¹H, ¹¹B and ¹³C NMR spectra in DMSO-d6 were used to confirm the product obtained by this method was identical to that obtained for Method C.

References:

Slabber, Cathryn A.;Grimmer, Craig D.;Robinson, Ross S. [Journal of Organometallic Chemistry,2013,vol. 723,p. 122 - 128]

1214264-88-6 Synthesis