ChemicalBook CAS DataBase List 6-bromo-3,3-dimethyl-1H-pyrrolo[3,2-b]pyridin-2(3H)-one

6-bromo-3,3-dimethyl-1H-pyrrolo[3,2-b]pyridin-2(3H)-one synthesis

2synthesis methods

Product Name:6-bromo-3,3-dimethyl-1H-pyrrolo[3,2-b]pyridin-2(3H)-one
CAS Number:1190862-33-9
Molecular formula:C9H9BrN2O
Molecular Weight:241.08

methyl 2-(5-bromo-3-nitropyridin-2-yl)-2-methylpropanoate

1259512-10-1
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6-bromo-3,3-dimethyl-1H-pyrrolo[3,2-b]pyridin-2(3H)-one

1190862-33-9
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Yield: 83%

Reaction Conditions:

with iron in acetic acid at 100; for 0.75 h;Inert atmosphere;

References:

Gonzalez-Lopez De Turiso, Felix;Shin, Youngsook;Brown, Matthew;Cardozo, Mario;Chen, Yi;Fong, David;Hao, Xiaolin;He, Xiao;Henne, Kirk;Hu, Yi-Ling;Johnson, Michael G.;Kohn, Todd;Lohman, Julia;McBride, Helen J.;McGee, Lawrence R.;Medina, Julio C.;Metz, Daniela;Miner, Kent;Mohn, Deanna;Pattaropong, Vatee;Seganish, Jennifer;Simard, Jillian L.;Wannberg, Sharon;Whittington, Douglas A.;Yu, Gang;Cushing, Timothy D. [Journal of Medicinal Chemistry,2012,vol. 55,# 17,p. 7667 - 7685]

99365-40-9
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74-88-4
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References