6,6-dimethyl-1-methylidene-4,8-dioxaspiro[2.5]oct ane synthesis

5synthesis methods

Product Name:6,6-dimethyl-1-methylidene-4,8-dioxaspiro[2.5]oct ane
CAS Number:122968-05-2
Molecular formula:C9H14O2
Molecular Weight:154.21

4,8-Dioxaspiro[2.5]oct-1-ene, 1,6,6-trimethyl-

122762-81-6
0 suppliers
inquiry

6,6-dimethyl-1-methylidene-4,8-dioxaspiro[2.5]oct ane

122968-05-2
2 suppliers
inquiry

Yield:122968-05-2 79%

Reaction Conditions:

with potassium tert-butylate;tert-butyl alcohol in diethyl ether at -78 - 20; for 4 h;Inert atmosphere;

References:

Nakamura, Masaharu;Wang, Xiao Qun;Isaka, Masahiko;Yamago, Shigeru;Nakamura, Eiichi;Wu, Jimmy;Grabowski, Edward J. J. [Organic Syntheses,2003,vol. 80,p. 144 - 159]

6,6-Dimethyl-4,8-dioxaspiro[2.5]oct-1-ene

60935-22-0
1 suppliers
inquiry

122968-05-2
2 suppliers
inquiry

References

2,2-bis(chloromethyl)-5,5-dimethyl-1,3-dioxane

133961-12-3
1 suppliers
inquiry

74-88-4
342 suppliers
$15.00/10g

122968-05-2
2 suppliers
inquiry

References

133961-12-3
1 suppliers
inquiry

122968-05-2
2 suppliers
inquiry

References

126-30-7 Synthesis

126-30-7
612 suppliers
$8.00/100g

122968-05-2
2 suppliers
inquiry

References