ChemicalBook CAS DataBase List 1,4-BIS-[4-(6-ACRYLOYLOXYHEXYLOXY)BENZOYLOXY]-2-METHYLBENZENE

1,4-BIS-[4-(6-ACRYLOYLOXYHEXYLOXY)BENZOYLOXY]-2-METHYLBENZENE synthesis

5synthesis methods

Product Name:1,4-BIS-[4-(6-ACRYLOYLOXYHEXYLOXY)BENZOYLOXY]-2-METHYLBENZENE
CAS Number:125248-71-7
Molecular formula:C39H44O10
Molecular Weight:672.77

1,4-Bis-[4-(6-acryloyloxyhexyloxy)benzoyloxy]-2-Methylbenzene can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process. Its synthesis method is as followed: 2-Methylhydroquinone and 4-(6-Prop-2-enoyloxyhexoxy)benzoic acid with dmap, dicyclohexyl-carbodiimide in dichloromethane was stirred for 48 h and give to the finished product.

2009-83-8 Synthesis

2009-83-8
358 suppliers
$7.00/25g

1,4-BIS-[4-(6-ACRYLOYLOXYHEXYLOXY)BENZOYLOXY]-2-METHYLBENZENE

125248-71-7
135 suppliers
$6.00/250mg

Yield:-

Steps:

Multi-step reaction with 4 steps
1: sodium hydroxide; potassium iodide / acetone / 20 h / 60 °C
2: potassium hydroxide / water / 6 h / 60 °C
3: N,N-dimethyl-aniline / 1,4-dioxane / 3 h / 60 °C
4: dicyclohexyl-carbodiimide; dmap / dichloromethane / 48 h

References:

Chen, Xingwu;Wang, Ling;Chen, Yinjie;Li, Chenyue;Hou, Guoyan;Liu, Xin;Zhang, Xiaoguang;He, Wanli;Yang, Huai [Chemical Communications,2014,vol. 50,# 6,p. 691 - 694]

FullText

95-71-6 Synthesis