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ChemicalBook CAS DataBase List Ethanol, 2-[2-[2-[(6-chlorohexyl)oxy]ethoxy]ethoxy]-

Ethanol, 2-[2-[2-[(6-chlorohexyl)oxy]ethoxy]ethoxy]- synthesis

2synthesis methods
2163-00-0 Synthesis
1,6-Dichlorohexane

2163-00-0
332 suppliers
$7.00/25g

Ethanol, 2-[2-[2-[(6-chlorohexyl)oxy]ethoxy]ethoxy]-

1355955-95-1
12 suppliers
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Yield:1355955-95-1 68%

Reaction Conditions:

Stage #1: 2,2'-[1,2-ethanediylbis(oxy)]bisethanol in benzene; for 2 h;Reflux;Dean-Stark receiver;
Stage #2: with sodium in benzene;Dean-Stark receiver;
Stage #3: 1,6-dichlorohexane in benzene; for 4 h;Reflux;

References:

Matijoska, Algirdas;Charkova, Tatjana;Kuodis, Zenonas;Voiciuk, Vladislava;Eicher-Lorka, Olegas [Central European Journal of Chemistry,2012,vol. 10,# 1,p. 113 - 120] Location in patent:experimental part