2-(2-[3,5-BIS(TRIFLUOROMETHYL)PHENYL]HYDRAZONO)MALONONITRILE synthesis
- Product Name:2-(2-[3,5-BIS(TRIFLUOROMETHYL)PHENYL]HYDRAZONO)MALONONITRILE
- CAS Number:138555-70-1
- Molecular formula:C11H4F6N4
- Molecular Weight:306.17
Yield:138555-70-1 70%
Reaction Conditions:
Stage #1: 3,5-Bis-(trifluoromethyl)anilinewith hydrogenchloride;sodium nitrite in water; for 1.5 h;Cooling with ice;
Stage #2: malononitrilewith sodium acetate in water at 0; for 2 h;
References:
Lu, Jun;Lu, Xueer;Tang, Wenjian;Xu, Yingying;Zhang, Jing;Zhang, Ziwen [RSC Advances,2020,vol. 10,# 30,p. 17854 - 17861]
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138555-70-1
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