(3,5-DIMETHYLPHENYL)HYDRAZINE HYDROCHLORIDE synthesis
- Product Name:(3,5-DIMETHYLPHENYL)HYDRAZINE HYDROCHLORIDE
- CAS Number:39943-61-8
- Molecular formula:C8H12N2
- Molecular Weight:136.19
108-69-0
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39943-61-8
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Yield:39943-61-8 76%
Reaction Conditions:
Stage #1: 3,5-dimethylaminoanilinewith hydrogenchloride;sodium nitrite in water at -10; for 0.5 h;Inert atmosphere;
Stage #2: with tin(ll) chloride in water at -10 - 20; for 0.5 h;
References:
Narlawar, Rajeshwar;Werry, Eryn L.;Scarf, Alana M.;Hanani, Raphy;Chua, Sook Wern;King, Victoria A.;Barron, Melissa L.;Martins, Ralph N.;Ittner, Lars M.;Rendina, Louis M.;Kassiou, Michael [Journal of Medicinal Chemistry,2015,vol. 58,# 21,p. 8743 - 8749] Location in patent:supporting information
60481-36-9
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39943-61-8
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556-96-7
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$6.00/5g
39943-61-8
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