3-Methoxy-4-methylphenylboronic acid, pinacol ester synthesis
- Product Name:3-Methoxy-4-methylphenylboronic acid, pinacol ester
- CAS Number:1417036-28-2
- Molecular formula:C14H21BO3
- Molecular Weight:248.13
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Yield:-
Reaction Conditions:
with (6,6’-dimethoxy-[1,1 ‘-biphenyl]-2,2’-diyl)bis(bis(3 ,5-dimethyl-phenyl)phosphine);[Ir(OH)(cod)]2 in hexane at 85; for 20 h;Inert atmosphere;Glovebox;Sealed tube;Overall yield = 86 %; Overall yield = 107 mg; regioselective reaction;
References:
Saito, Yutaro;Segawa, Yasutomo;Itami, Kenichiro [Journal of the American Chemical Society,2015,vol. 137,# 15,p. 5193 - 5198] Location in patent:supporting information