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ChemicalBook CAS DataBase List C-(4-ALLYL-MORPHOLIN-2-YL)-METHYLAMINE DIHYDROCHLORIDE

C-(4-ALLYL-MORPHOLIN-2-YL)-METHYLAMINE DIHYDROCHLORIDE synthesis

2synthesis methods
Acetamide, N-[[4-(phenylmethyl)-2-morpholinyl]methyl]-

112913-96-9
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C-(4-ALLYL-MORPHOLIN-2-YL)-METHYLAMINE DIHYDROCHLORIDE

141815-17-0
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: H2 / 10percent Pd/C / ethanol; acetic acid / 60 °C
2: K2CO3, KI / butan-2-one / 17 h / Heating
3: 10percent NaOH / 20 h / Heating

References:

Kato;Morie;Harada;Yoshida;Matsumoto [Chemical and Pharmaceutical Bulletin,1992,vol. 40,# 3,p. 652 - 660]

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