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tert-butyl 3-(2-hydroxyethyl)-1H-indole-1-carboxylate synthesis

11synthesis methods
786647-50-5 Synthesis
Ethyl N-Boc-(indol-3-yl)acetate/tert-butyl 3-(2-ethoxy-2-oxoethyl)-1H-indole-1-carboxylate

786647-50-5
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tert-butyl 3-(2-hydroxyethyl)-1H-indole-1-carboxylate

141972-32-9
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Yield:141972-32-9 493 mg

Reaction Conditions:

with lithium aluminium tetrahydride in tetrahydrofuran at 0; for 0.0833333 h;Inert atmosphere;

References:

Sato, Shigeki;Shibuya, Masatoshi;Kanoh, Naoki;Iwabuchi, Yoshiharu [Chemical Communications,2009,# 41,p. 6264 - 6266] Location in patent:supporting information; experimental part

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