2-(Dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-Imidazole synthesis
- Product Name:2-(Dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-Imidazole
- CAS Number:1425052-90-9
- Molecular formula:C22H31N2OP
- Molecular Weight:370.47
90-04-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: ammonium acetate / acetic acid; water / 70 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -30 °C / Inert atmosphere
2.2: 2.5 h / -30 - 50 °C / Inert atmosphere
References:
Aspin, Sam;Lopez-Suarez, Laura;Larini, Paolo;Goutierre, Anne-Sophie;Jazzar, Rodolphe;Baudoin, Olivier [Organic Letters,2013,vol. 15,# 19,p. 5056 - 5059]
