ChemicalBook CAS DataBase List 3-(4-Fluobenzenesulfhydry)-2-hydroxyl-2-methylpropionic acid

3-(4-Fluobenzenesulfhydry)-2-hydroxyl-2-methylpropionic acid synthesis

2synthesis methods

Product Name:3-(4-Fluobenzenesulfhydry)-2-hydroxyl-2-methylpropionic acid
CAS Number:151262-57-6
Molecular formula:C10H11FO5S
Molecular Weight:262.25

Benzene, 1-fluoro-4-[(2-methyl-2-propen-1-yl)sulfonyl]-

104517-36-4
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3-(4-Fluobenzenesulfhydry)-2-hydroxyl-2-methylpropionic acid

151262-57-6
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; tert-butyl alcohol / 8 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium chlorite; sodium hypochlorite / acetonitrile; aq. phosphate buffer; water / 74 h / 35 °C / pH 6.7 / Inert atmosphere; Schlenk technique

References:

Jhang, Yin-Jia;Chang, Chieh-Yu;Lin, Yu-Huan;Lee, Chein-Chung;Wu, Yen-Ku [Tetrahedron Letters,2021,vol. 73,art. no. 153060]

824-80-6 Synthesis

4-FLUOROBENZENESULFINIC ACID SODIUM SALT

824-80-6
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References

3-(4-Fluobenzenesulfhydry)-2-hydroxyl-2-methylpropionic acid Related Search:

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