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155396-71-7 synthesis

6synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
823 suppliers
$13.50/25G

155396-71-7

155396-71-7
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: ammonium hydroxide / ethanol; water / 18.58 h / -10 - 20 °C
2: water; methanol; formic acid / 72 h / 20 °C

References:

Best, Daniel;Kujawa, Szymon;Lam, Hon Wai [Journal of the American Chemical Society,2012,vol. 134,# 44,p. 18193 - 18196]