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ChemicalBook CAS DataBase List 2-PYRIDINECARBALDEHYDE N-[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]HYDRAZONE

2-PYRIDINECARBALDEHYDE N-[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]HYDRAZONE synthesis

2synthesis methods
-

Yield:173213-31-5 52%

Steps:

29 Synthesis of 2-pyridinecarbaldehyde-(3-chloro-5-trifluoromethyl-2-pyridyl)hydrazone (compound 29)

EXAMPLE 29 Synthesis of 2-pyridinecarbaldehyde-(3-chloro-5-trifluoromethyl-2-pyridyl)hydrazone (compound 29) A desired product was obtained in the same manner as in Example 1 by using 4.30 g (20.3 mmol) of 3-chloro-5-trifluoromethyl-2-pyridylhydrazine and 2.0 ml (2.25 g, 21.0 mmol) of 2-pyridinecarbaldehyde. Yield: 3.20 g (10.6 mmol) [yield rate: 52%] Melting point: 225° to 226° C.

References:

US5569763,1996,A