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ChemicalBook CAS DataBase List 4-Methoxyphenyl 4,6-O-Benzylidene-beta-D-galactopyranoside

4-Methoxyphenyl 4,6-O-Benzylidene-beta-D-galactopyranoside synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: boron trifluoride diethyl etherate / dichloromethane / 24 h / 20 °C / Ionic liquid
2: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere
3: toluene-4-sulfonic acid / acetonitrile / Inert atmosphere

References:

Gampe, Christian M.;Tsukamoto, Hirokazu;Doud, Emma H.;Walker, Suzanne;Kahne, Daniel [Journal of the American Chemical Society,2013,vol. 135,# 10,p. 3776 - 3779]

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