(3-BENZYLAMINO-1-METHYL-PROPYL)-CARBAMIC ACID TERT-BUTYL ESTER synthesis

4synthesis methods

Product Name:(3-BENZYLAMINO-1-METHYL-PROPYL)-CARBAMIC ACID TERT-BUTYL ESTER
CAS Number:176982-58-4
Molecular formula:C16H26N2O2
Molecular Weight:278.39

79069-13-9
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(3-BENZYLAMINO-1-METHYL-PROPYL)-CARBAMIC ACID TERT-BUTYL ESTER

176982-58-4
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 86 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C
2: 72 percent / dimethylsulfoxide / 15 h / 40 - 45 °C
3: 94 percent / H₂; NH₃ / Raney Ni / ethanol / 15 h / 20 °C / 4500.36 Torr
4: 98 percent / 3 Angstroem molecular sieves / diethyl ether / 20 h / 20 °C
5: 84 percent / NaBH₄ / ethanol / 3 h / 10 °C

References:

Lebreton, Luc;Jost, Eric;Carboni, Bertrand;Annat, Jocelyne;Vaultier, Michel;Dutartre, Patrick;Renaut, Patrice [Journal of Medicinal Chemistry,1999,vol. 42,# 23,p. 4749 - 4763]

(S)-Methanesulphonic acid 2-Boc-aminopropyl ester

126301-16-4
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176982-58-4
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References

172695-22-6 Synthesis

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176982-58-4
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References

176982-57-3
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176982-58-4
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References

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