n-methoxy-n-methyl-succinamic acid tert-butyl ester synthesis
- Product Name:n-methoxy-n-methyl-succinamic acid tert-butyl ester
- CAS Number:180858-08-6
- Molecular formula:C10H19NO4
- Molecular Weight:217.26
15026-17-2
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6638-79-5
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180858-08-6
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Yield:180858-08-6 100%
Reaction Conditions:
Stage #1: succinic acid mono-tert-butyl esterwith 1,1'-carbonyldiimidazole in dichloromethane at 20; for 1 h;Inert atmosphere;
Stage #2: N,O-dimethylhydroxylamine*hydrochloride in dichloromethane at 20;Inert atmosphere;
References:
Choi, Shinyoung;Dong, Guangbin;Liu, Xin;Xie, Jiaxin;Zhang, Nan [Journal of the American Chemical Society,2021,vol. 143,# 46,p. 19311 - 19316] Location in patent:supporting information
15026-17-2
150 suppliers
$6.00/1g
180858-08-6
12 suppliers
inquiry